16.4     Detrital populations

 

An advantage of the external detector method of fission track counting is the ability to determine a separate age from each grain of the population (this also applies to the less-widely used re-polishing method). This capability is useful if a heterogeneous age population is suspected in the sample, as in the case of sedimentary rocks with mixed provenance (e.g. Hurford and Carter, 1991). However, the scatter of analysis points generated by these kinds of sample can be a challenge when it comes to data presentation. 

 

            Fission track results for individual detrital grains may be presented in histogram form. However, a more quantitative age estimate is possible if errors are assigned to each individual grain determination, so that the data can be presented as a probability density function (Hurford et al., 1984). This function is simply the summation of the Poisson age distributions for each of the individual grain determinations. Fig. 16.9 shows such a plot for zircons from the re-worked El Ocote tephra deposit in Mexico, which displays a bimodal age distribution (Kowallis et al., 1986). The younger peak places a maximum age on the time of sedimentary re-working, and is in agreement with the estimated biostratigraphic age of associated fossil material. These results show that application of the population method to fission track dating of this tephra would yield a meaningless average of the two age populations.

Fig. 16.9. Plot of probability density as a function of age for fission track data on detrital zircons from the re-worked El Ocote tephra from Mexico. After Kowallis et al. (1986).

 

            A problem with the probability density plot is that individual data points cannot be distinguished, so that some important but small components in the data distribution can be buried under the other data. To avoid these problem, Galbraith (1988) introduced a kind of isochron diagram for the presentation of fission track data measured on individual grains of a heterogeneous sample.  This ‘radial’ plot is designed for fission track data sets with a high degree of scatter, either due to mixed detrital ages or variable cooling ages.

 

            This diagram differs from other isochron plots used in geology because the two variables plotted are the apparent fission track age of each grain, and the standard error of each grain age (F). These quantities are plotted in the form of age/F against 1/F (Fig. 16.10a). In this plot, the slope of an array indicates the average age of the suite of grains analysed, and this age can be indicated on a calibrated arc. In practice, Galbraith argued, it is more convenient to normalise the average slope to a horizontal, and plot the y axis on a log scale from +2 to 2 (Fig. 16.10b). The age of any individual point is then determined by projecting from the zero point on the y axis, through the data point, to the calibrated arc of ages (on a log scale).

Fig. 16.10. Variations on the radial plot for presentation of single grain fission track data on heterogeneous samples; a) raw data; b) normalised. After Galbraith (1988).

 

            An alternative data presentation of this type was proposed by Walter (1989). He suggested that additional assessments could be made of the quality of detrital fission track ages if the raw data (spontaneous- versus induced-track densities) were plotted for each grain. This also yields an isochron diagram (Fig. 16.11) where the slope of each correlation line is proportional to age. These lines should pass through the origin, corresponding to a grain with zero uranium content. The linearity of each correlation line can be used to assess the influence of systematic analytical errors or geological disturbance on the reliability of the best-fit ages. However, this presentation has not been as popular as the isochron diagram of Galbraith, which has found wide application to complex fission track data sets, including partially annealed systems as well as detrital systems.

Fig. 16.11. Spontaneous- versus induced-track isochron diagram showing data for individual zircon grains from the El Ocote tephra. After Walter (1989).

 

 

References

 

Bhandari, N. Bhat, S. G., Rajogopalan, G., Tamhane, A. S. and Venkatavaradan, V. S. (1971). Fission fragment lengths in apatite: recordable track lengths. Earth Planet. Sci. Lett. 13, 191)9.

 

Bigazzi, G. (1967). Length of fission tracks and age of muscovite samples. Earth Planet. Sci. Lett. 3, 434)8.

 

Briggs, N. D., Naeser, C. W. and McCulloh, T. H. (1981). Thermal history of sedimentary basins by fission-track dating. Nucl. Tracks 5, 235)7 (abstract).

 

Carlson, W. D. (1990). Mechanisms and kinetics of apatite fission-track annealing. Amer. Miner. 75, 112039.

 

Corrigan, J. (1991). Inversion of apatite fission track data for thermal history information. J. Geophys. Res. 96, 10 34760.

 

Crowley, K. D., Cameron, M. and Schaefer, R. L. (1991). Experimental studies of annealing of etched fission tracks in fluorapatite. Geochim. Cosmochim. Acta 55, 144965.

 

Dakowski, M. (1978). Length distributions of fission tracks in thick crystals. Nucl. Track Det. 2, 181)9.

 

Duddy, I. R., Green, P. F. and Laslett, G. M. (1988). Thermal annealing of fission tracks in apatite 3. Variable temperature behaviour. Chem. Geol. (Isot. Geosci. Sect.) 73, 2538.

 

Fleischer, R. L. and Hart, H. R. (1972). Fission track dating: techniques and problems. In: Bishop, W., Miller, J. and Cole, S. (Eds), Calibration of Hominoid Evolution. Scottish Academic Press, pp. 135)170.

 

Fleischer, R. L. and Price, P. B. (1964a). Techniques for geological dating of minerals by chemical etching of fission fragment tracks. Geochim. Cosmochim. Acta 28, 1705)14.

 

Fleischer, R. L. and Price, P. B. (1964b). Glass dating by fission fragment tracks. J. Geophys. Res. 69, 331)9.

 

Fleischer, R. L., Price, P. B., Symes, E. M. and Miller, D. S. (1964). Fission track ages and track-annealing behaviour of some micas. Science 143, 349)51.

 

Fleischer, R. L., Price, P. B. and Walker, R. M. (1965a). Tracks of charged particles in solids. Science 149, 383)93.

 

Fleischer, R. L., Price, P. B. and Walker, R. M. (1965b). Effects of temperature, pressure, and ionization on the formation and stability of fission tracks in minerals and glasses. J. Geophys. Res. 70, 1497)502.

 

Fleischer, R. L., Price, P. B. and Walker, R. M. (1968). Charged particle tracks: tools for geochronology and meteor studies. In: Hamilton, E. and Farquhar, R. M. (Eds), Radiometric Dating for Geologists. Wiley Interscience, pp. 417)435.

 

Fleischer, R. L., Price, P. B. and Walker, R. M. (1975). Nuclear Tracks in Solids. University of California Press, 605 p.

 

Galbraith, R. F. (1988). Graphical display of estimates having differing standard errors. Tectonometrics 30, 27181.

 

Gallagher, K. (1995). Evolving temperature histories from apatite fission-track data. Earth Planet. Sci. Lett. 136, 42135.

 

Gleadow, A. J. W. and Duddy, I. R. (1981). A natural long-term track annealing experiment for apatite. Nucl. Tracks 5, 169)74.

 

Gleadow, A. J. W., Duddy, I. R., Green, P. F. and Lovering, J. F. (1986). Confined fission track lengths in apatite: a diagnostic tool for thermal history analysis. Contrib. Mineral. Petrol. 94, 405)15.

 

Gleadow, A. J. W., Duddy, I. R. and Lovering, J. F. (1983). Apatite fission-track analysis as a paleotemperature indicator for hydrocarbon exploration. Aust. Petrol. Explor. Soc. J. 23, 93–102.

 

Green, P. F. (1981). ‘Track-in track’ length measurements in annealed apatites. Nucl. Tracks 5, 121)8.

 

Green, P. F., Duddy, I. R., Gleadow, A. J. W. and Tingate, P. R. (1985). Fission-track annealing in apatite: track length measurements and the form of the Arrhenius plot. Nucl. Tracks 10, 323)8.

 

Green, P. F., Duddy, I. R., Gleadow, A. J. W., Tingate, P. R. and Laslett, G. M. (1986). Thermal annealing of fission tracks in apatite. 1. A qualitative description. Chem. Geol. (Isot. Geosci. Sect.) 59, 23753.

 

Green, P. F., Duddy, I. R., Laslett, G. M., Hegarty, K. A., Gleadow, A. J. W. and Lovering, J. F. (1989). Thermal annealing of fission tracks in apatite 4. Quantitative modelling techniques and extension to geological timescales. Chem. Geol. (Isot. Geosci. Section) 79, 155)82.

 

Green, P. F. and Durrani, S. A. (1977). Annealing studies of tracks in crystals. Nucl. Track Det. 1, 33)9.

 

Green, P. F., Laslett, G. M. and Duddy, I. R. (1993). Mechanisms and kinetics of apatite fission-track annealing Discussion. Amer. Miner. 78, 4415.

 

Hejl, E. (1995). Evidence for unetchable gaps in apatite fission tracks. Chem. Geol. (Isot. Geosci. Sect.) 122, 25969.

 

Hurford, A. J. (1990). Standardization of fission track calibration: recommendation by the Fission Track Working Group of the I.U.G.S. Subcommission on Geochronology. Chem. Geol. (Isot. Geosci. Section) 80, 171)8.

 

Hurford, A. J. and Carter, A. (1991). The role of fission track dating in discrimination of provenance. In: Morton, A. C., Todd, S. P. and Haughton, P. D. W. (Eds) Developments in Sedimentary Provenance Studies. Geol. Soc. Spec. Pub. 57, 67)78.

 

Hurford, A. J., Fitch, F. J. and Clarke, A. (1984). Resolution of the age structure of the detrital zircon populations of two Lower Cretaceous sandstones from the Weald of England by fission track dating. Geol. Mag. 121, 269)77.

 

Hurford, A. J. and Green, P. F. (1982). A users’ guide to fission track dating calibration. Earth Planet. Sci. Lett. 59, 343)54.

 

Hurford, A. J. and Green, P. F. (1983). The . age calibration of fission-track dating. Isot. Geosci. 1, 285)317.

 

Kowallis, B. J., Heaton, J. S. and Bringhurst, K. (1986). Fission-track dating of volcanically derived sedimentary rocks. Geology 14, 19)22.

 

Lal, D., Rajan, R. S. and Tamhane, A. S. (1969). Chemical composition of nuclei of Z > 22 in cosmic rays using meteoritic minerals as detectors. Nature 221, 33)7.

 

Laslett, G. M., Galbraith, R. F. and Green, P. F. (1994). The analysis of projected fission track lengths. Rad. Meas. 23, 10323.

 

Laslett, G. M., Gleadow, A. J. W. and Duddy, I. R. (1984). The relationship between fission track length and track density in apatite. Nucl. Tracks 9, 29)37.

 

Laslett, G. M., Green, P. F., Duddy, I. R. and Gleadow, A. J. W. (1987). Thermal annealing of fission tracks in apatite, 2. A quantitative analysis. Chem. Geol. (Isot. Geosci. Section) 65, 1)13.

 

Laslett, G. M., Kendall, W. S., Gleadow, A. J. W. and Duddy, I. R. (1982). Bias in measurement of fission-track length distributions. Nucl. Tracks 6, 79)85.

 

Maurette, M., Pellas, P. and Walker, R. M. (1964). Etude des traces fission fossiles dans le mica. Bull. Soc. Franc. Miner. Cryst. 87, 6)17.

 

Naeser, C. W. (1979a). Fission-track dating and geological annealing of fission tracks. In: Jager, E. and Hunziker, J. C. (Eds), Lectures in Isotope Geology. Springer-Verlag, pp. 154)69.

 

Naeser, C. W. (1979b). Thermal history of sedimentary basins: Fission-track dating of subsurface rocks. In: Scholle, P. A., and Schluger, P. R. (Eds), Aspects of Diagenesis. Soc. Econ. Paleontol. Mineral. Spec. Pub. 26, pp. 109)12.

 

Naeser, C. W. (1981). The fading of fission tracks in the geologic environment) data from deep drill holes. Nucl. Tracks. 5, 248)50 (abstract).

 

Naeser, C. W. and Faul, H. (1969). Fission track annealing in apatite and sphene. J. Geophys. Res. 74, 705)10.

 

Naeser, C. W., Zimmermann, R. A. and Cebula, G. T. (1981). Fission-track dating of apatite and zircon: an inter-laboratory comparison. Nucl. Tracks 5, 65)72.

 

Naeser, N. D. and Naeser, C. W. (1984). Fission-track dating. In: Mahaney, W. C. (Ed.), Quaternary Dating Methods. Developments in Paleontology and Stratigraphy 7. Elsevier, pp. 87)100.

 

Naeser, N. D., Naeser, C. W. and McCulloh, T. H. (1989). The application of fission-track dating to the depositional and thermal history of rocks in sedimentary basins. In: Naeser, N. D. and McCulloh, T. H. (Eds), Thermal History of Sedimentary Basins. Springer-Verlag, pp. 157)80.

 

Price, P. B. and Walker, R. M. (1962a). Chemical etching of charged particle tracks in solids. J. Appl. Phys. 33, 3407)12.

 

Price, P. B. and Walker, R. M. (1962b). Observation of fossil  particle tracks in natural micas. Nature 196, 732)4.

 

Price, P. B. and Walker, R. M. (1963). Fossil tracks of charged particles in mica and the age of minerals. J. Geophys. Res. 68, 4847)62.

 

Reimer, G. M., Storzer, D. and Wagner, G. A. (1970). Geometry factor in fission track counting. Earth Planet. Sci. Lett. 9, 401)4.

 

Silk, E. C. H. and Barnes, R. S. (1959). Examination of fission fragment tracks with an electron microscope. Phil. Mag. 4, 970)2.

 

Storzer, D. and Poupeau, G. (1973). Ages plateaux de mineraux et verres par la methode des traces de fission. C. R. Acad. Sci. Paris 276, 137)9.

 

Storzer, D. and Wagner, G. A. (1969). Correction of thermally lowered fission track ages of tektites. Earth Planet. Sci. Lett. 5, 463)8.  CHECK THIS!

 

Storzer, D. and Wagner, G. A. (1982). The application of fission track dating in stratigraphy: a critical review. In: Odin, G. S. (Ed.), Numerical Dating in Stratigraphy. Wiley, pp. 199)221.

 

Wagner, G. A. (1978). Archaeological applications of fission-track dating. Nucl. Track Det. 2, 51)63.

 

Wagner, G. A. (1988). Apatite fission-track geochrono-thermometer to 60 oC: projected length studies. Chem. Geol. (Isot. Geosci. Section) 72, 145)53.

 

Wagner, G. A. and Hejl, E. (1991). Apatite fission-track age-spectrum based on projected track-length analysis. Chem. Geol. (Isot. Geosci. Section) 87, 1)9.

 

Wagner, G. A. and Reimer, G. M. (1972). Fission-track tectonics: the tectonic interpretation of fission track apatite ages. Earth Planet. Sci. Lett. 14, 263)8.

 

Wagner, G. A., Reimer, G. M. and Jager, E. (1977). Cooling ages derived by apatite fission-track, mica Rb)Sr and K)Ar dating: the uplift and cooling history of the Central Alps. Mem. Inst. Geol. Min. Univ. Padova 30, 1)27.

 

Walter, R. C. (1989). Application and limitation of fission-track geochronology to Quaternary tephras. Quat. Int. 1, 35)46.

 

Wendt, A. S., Vidal, O. and Chadderton, L. T. (2002). Experimental evidence for the pressure dependence of fission track annealing in apatite. Earth Planet. Sci. Lett. 201, 593–607.